WANG Li-xia,LIU Kun.Extraction Technology on Flavonoids From Corn Silk by Ultrasonic-assisted[J].Northern Horticulture,2014,38(06):137-139.
超声波辅助提取玉米须黄酮工艺
- Title:
- Extraction Technology on Flavonoids From Corn Silk by Ultrasonic-assisted
- 文章编号:
- 1001-0009(2014)06-0137-03
- Keywords:
- corn silk; flavonoids; ultrasonic extraction
- 分类号:
- S 513
- 文献标志码:
- A
- 摘要:
- 以玉米须为试材,以乙醇溶液为提取剂,通过单因素和L9(34)正交实验,分别对乙醇的浓度、料液比、超声温度、超声时间4因素进行了优化组合,以总黄酮提取量为评价指标,研究了超声波辅助提取优选玉米须中的黄酮类物质的最佳工艺条件。结果表明:总黄酮类物质的最佳提取工艺为乙醇浓度40%,料液比1∶40 g/mL,超声温度60℃,超声时间5 min,此条件下黄酮提取率为0.301%。
- Abstract:
- With corn silk as material,the flavonoid extracted from corn silk was stuided by ultrasonic extraction,with the alcohol as extracting agent,the alcohol content,material liquid ratio,ultrasonic temperature and ultrasonic time were optimized by single factors and L9(34) orthogonal experiment.The flavone was defined as the amount of extraction.The results showed that the optimal extraction process of flavonoid was material liquid ratio 1∶40 g/mL,alcohol solvent 40%,ultrasonic temperature 60℃ for 5 min,the rate of extraction was 0.301% under this condition.
参考文献/References:
[1]张育光.玉米须化学成分、药理作用及其应用研究进展[J].中国中医药现代远程教育,2007,5(2):34-35. [2]匡轩,匡芮,朱海涛.玉米须的化学成分及药理保健功能[J].中国食物与营养,2007(4):46-48. [3]Weight control drug products for over-the 2-counter human use,certain active ingredients fed regist[J].Food and Drag Adminstration USA,1991,56(153):397792. [4]曹纬国,刘志勤,邵云,等.黄酮类化合物药理作用的研究进展[J].西北植物学报,2003(12):2241-2246. [5]国家药典委员会编.中国药典[S].附录VA.北京:化学工业出版社,2005. [6]许钢.玉米不同部位提取物抗氧化性能比较[J].食品与发酵工业,2004,30(4):88-92. [7]Snook M E.New C-4-hydroxy derivatives of may sin and 3’-metalhoxy may sin isolated from silks (Zes mays)[J].Agric Food Chem,1995,43:2740-2745. [8]胡爱军,郑捷.食品工业中的超声提取技术[J].食品与机械,2004(4):57-60. [9]苏东林,单杨,李高阳.紫外分光光度法测定玉米须中总黄酮的含量[J].食品研究与开发,2007(8):124-128. [10]任顺成,丁霄霖.玉米须黄酮类测定方法的研究[J].食品科学,2004(3):139-142. [11]黄丹,严芳,钟世荣,等.超声波辅助水提紫苏活性成分工艺优化研究[J].中国食品添加剂,2010(4):161-164.
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备注/Memo
第一作者简介:王丽霞(1981-),女,硕士,讲师,研究方向为食品加工技术。E-mail:wanglixia04216@163.com.