WANG Yuan-yuan,ZHAO Bing-kun,GUO Yan-yin,et al.Study on Optimization Process of Ginger Oil by Solvent Extraction[J].Northern Horticulture,2014,38(11):130-134.
溶剂提取生姜油的工艺优化研究
- Title:
- Study on Optimization Process of Ginger Oil by Solvent Extraction
- 文章编号:
- 1001-0009(2014)11-0130-05
- Keywords:
- ginger; ginger oil; ginger powder; petroleum ether; solvent; extraction
- 分类号:
- S 632.5
- 文献标志码:
- A
- 摘要:
- 以生姜为试材，采用石油醚（沸程60~90℃）、环己烷、乙醚、正戊烷4种萃取剂，研究了生姜干鲜材料、物料粒度、料液比、萃取温度、蒸馏温度等因素对生姜油萃取率的影响，以期研究溶剂提取生姜油的最佳工艺。结果表明：单因素试验条件下，石油醚为生姜油的适宜萃取剂，过60目筛的干姜粉较适于生姜油的提取，料液比为1∶3 g/mL、萃取温度45℃和0.7 kPa压力下蒸馏温度45℃适于生姜油的提取；正交实验表明，最佳优化工艺为萃取料液比1∶3.5 g/mL，萃取温度40℃，萃取时间30 min，在此工艺条件下，生姜油提取率为4.3%，且所得生姜油具有纯正的生姜风味。
- Abstract:
- Taking ginger as material,based on the screen of petroleum ether(boiling range 60~90℃),cyclohexane,aether and n-pentane,the effect of factors such as ginger dry/fresh material,material particle,material-liquid ratio,extraction temperature and distillation temperature on the extraction rate of ginger oil were investigated in order to study the best process in solvent extraction of ginger oil.The results showed that,under single factor experiment,petroleum ether was the optical extraction agent,dry ginger powder that through 60 meshes was suitable for ginger oil extraction,and the appropriate material/liquid ratio,extraction temperature,and distillation temperature under 0.7 kPa pressure was 1∶3 g/mL,extraction 45℃ and distillation 45℃,respectively.Further orthogonal experiment indicated that the optimal material/liquid ratio,extractation temperature,and extraction time was 1∶3.5 g/mL,extraction temperature 40℃,and extraction time 30 min,respectively.This process could improve the extraction rate to 4.3%,and the ginger oil extracted had pure ginger flavor.
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备注/Memo
第一作者简介：王媛媛（1987-），女，硕士研究生，研究方向为农产品贮藏与加工。E-mail：764260790@qq.com.
责任作者：郭衍银（1976-），男，副教授，现主要从事农产品贮藏与加工技术等研究工作。E-mail：guoyy@sdut.edu.cn.
收稿日期：2014-01-17