WEN Xin,WU Dongmei,LI Jinlian,et al.Compounds Analysis of Different Producing Areas From Essential Oil of Chrysanthemum[J].Northern Horticulture,2018,42(16):160-166.[doi:10.11937/bfyy.20180073]
不同产地雪菊挥发油化学成分比较
- Title:
- Compounds Analysis of Different Producing Areas From Essential Oil of Chrysanthemum
- 关键词:
- 雪菊; 挥发油; 成分; 气相色谱-质谱联用技术
- Keywords:
- chrysanthemum; essential oil; compound; GC-MS
- 文献标志码:
- A
- 摘要:
- 以黑龙江和新疆产地雪菊为试材，采用水蒸气蒸馏法提取雪菊挥发油，通过GC-MS联用技术鉴定雪菊挥发油成分，利用峰面积归一化法分析各成分占总含量的相对百分含量。结果表明：黑龙江雪菊挥发油中得到36个色谱峰，鉴定出23种化学成分，主要为柠檬烯（50.961%）、α-水芹烯（5.717%）、蒎烯（5.226%），新疆雪菊挥发油中得到36个色谱峰，鉴定出22种化学成分，主要为D-柠檬烯（59.911%），蒎烯（7.866%）、2-异丙基-5-甲基-9-亚甲基-双环[4.4.0]-1-癸烯（3.840%）；黑龙江雪菊经减压蒸馏处理，鉴定出的成分从23种减少到18种，主要成分为D-柠檬烯（65.810%）。柠檬烯和D-柠檬烯含量可作为鉴别2个产地雪菊挥发油的指标。
- Abstract:
- The composition of essential oil from different producing areas of chrysanthemum were determined and analyzed by GC-MS using steam distillation extraction and normalization method of peak area.The results showed that 36 chromatographicpeaks were found in Heilongjiang chrysanthemum essential oil,and 23 compounds were identified including limonene (50.961%),α-phellandrene (5.717%),(1R)-α-pinene (5.226%);36 chromatographic peaks were found in Xinjiang chrysanthemum essential oil,and 22 compounds were identified including D-limonene (59.911%),(1R)-α-pinene(7.866%),2,6-dimethyl-6-(4-methyl-3-pentenyl) bicyclo[3.1.1]hept-2-ene (3.840%).In the Heilongjiang chrysanthemum essential oil treated by vacuum distillation,18 compounds were identified including D-limonene (65.810%).There were obvious diversity in content and compound of chrysanthemum essential oil in different fields of the same variety,limonene and D-limonene could be used as identification index of chrysanthemum essential oil of Heilongjiang and Xinjiang.
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备注/Memo
第一作者简介：温馨（1992-），女，硕士研究生，研究方向为天然产物成分分析及抑菌活性。E-mail：1123315640@qq.com.责任作者：武冬梅（1967-），女，博士，教授，现主要从事天然产物种植及药理活性等研究工作。E-mail：dmwu@jmsu.edu.cn.基金项目：国家自然科学基金资助项目（21477048）;黑龙江省自然科学基金资助项目（B2017014）;佳木斯大学研究生科技创新资助项目（YZ2016_004）;佳木斯大学资助项目（22Zb201514）。收稿日期：2018-03-12