CHEN Ping,MIAO Xiao-yan,HE Fu-qiang.Study on Kinetics of Acid Hydrolysis and Extraction of Polysaccharide From Aloe[J].Northern Horticulture,2014,38(12):110-112.
芦荟多糖提取及酸水解动力学研究
- Title:
- Study on Kinetics of Acid Hydrolysis and Extraction of Polysaccharide From Aloe
- 文章编号:
- 1001-0009(2014)12-0110-03
- Keywords:
- aloe polysaccharide; extraction; acid hydrolysis kinetics
- 分类号:
- Q 949.9
- 文献标志码:
- A
- 摘要:
- 以新鲜库拉索芦荟为试材，采用改良的超声醇沉法提取芦荟多糖，并用旋光法测定了多糖在不同浓度HCl条件下水解反应动力学。结果表明：水解反应很好的符合一级动力学方程；改良的超声醇沉法简化了多糖提取工艺，耗能少，产率高，适用于实际生产；特别是用简单的旋光法测定的芦荟多糖的可控酸水解，为制备目标分子量规格的活性低聚糖奠定了理论基础。
- Abstract:
- Taking fresh Curacao aloe as material,polysaccharide was extracted by the optimized ultrasound alcohol sedimentation method,the polysaccharides was determinated in different concentration of HCl conditions with the optical method.The results showed that the hydrolysis reactions was coincidence with first grade equation.The optimized traditional alcohol sedimentation method was suitable for the industrial production because of simplified procedure and low energy consumption;these results would lay a theoretical foundation for the development application of aloe polysaccharide,especially in the preparation of active oligosaccharide with certain molecular under the acid-controllable conditions.
参考文献/References:
[1] 周媛,陈冬梅.芦荟的毒理研究进展[J].现代农业科技,2006(6):118-119.
[2] 李天东,罗英,李俊刚.芦荟多糖生物活性研究进展[J].安徽农业科学,2009,37(5):2033-2035.
[3] 于芳,胡云,彭常安,等.芦荟汁的抑菌作用[J].食品科学,2004,25 (10):77-80.
[4] Saini M,Goyal P K,Chaudhary G.Anti-tumor activity of Aloe Vera against DMBA/croton oil-induced skin papillomagenesis in Swiss albino mice [J].J Environ Pathol Toxicol Oncol,2010;29(2):127-135.
[5] 郑敏霞,丰素娟.芦荟的药用研究进展[J].浙江中医药大学学报,2006,30(3):313-315.
[6] 崔晏.苦瓜多糖和芦荟多糖的降血糖作用及其机理的研究[D].济南:山东师范大学,2003.
[7] 张素兰.芦荟多糖免疫调节作用研究进展[J].安徽农业科学,2009,37(32):15837-15839.
[8] 于洁,李威.含芦荟多糖与维生素E乳状化妆品的制备及其性能[J].日用化学工业,2007(4):281-282.
[9] 杨继远,袁仲.芦荟化学成分的保健功效与产品开发[J].农牧产品开发,2001(4):6-8.
[10] Lu Z Q,Deng Y J,Lu J X.Effect of aloe polysaccharide on caspase-3 expression following cerebral ischemia and reperfusion injury in rats[J].Molecular Medicine Reports,2012,6(2):371-374.
[11] 王俊玲,张丽芳,倪中海,等.芦荟多糖的提取及总糖含量测定[J].海峡药学,2002(5):57-69.
[12] 马稳,袁红霞.微波辅助提取芦荟中芦荟多糖的研究[J].食品科技,2008(9):162-168.
[13] 刘晓鹏,姜宁,向东山.库拉索芦荟多糖超声辅助提取工艺的研究[J].食品科学,2008,29(10):286-289.
[14] 张燕.白及多糖酸水解动力学研究[D].苏州:苏州大学,2010.
[15] 齐慧玲,魏绍云,王继伦.Sevag法去除白及多糖中蛋白的研究[J].天津化工,2000(3):20-21.
相似文献/References:
[1]张 虹,王景李,白红丽,等.云南翠雀花根中总黄酮提取方法的研究[J].北方园艺,2014,38(13):153.
ZHANG Hong,WANG Jing-li,BAI Hong-li,et al.Study on the Extraction Method Total Flavonoids in Root of the Delphinium yunnanense[J].Northern Horticulture,2014,38(12):153.
[2]罗 琴,林惠昆,管春平,等.正交实验法优化提取二型鳞毛蕨多糖工艺的研究[J].北方园艺,2013,37(22):146.
LUO Qin,LIN Hui-kun,GUAN Chun-ping,et al.Study on the Optimization of Extraction Technology of Polysaccharide from Dryopteris cochleata Using Orthogonal Experiment[J].Northern Horticulture,2013,37(12):146.
[3]邹家丽,邓骛远,和七一,等.山茶花中多酚提取的方法及其抗氧化活性测定研究[J].北方园艺,2013,37(13):103.
ZOU Jia-li,DENG Wu-yuan,HE Qi-yi,et al.Polyphenol Extracted from the Camellia japonica Flowers and Its Antioxidant Activity[J].Northern Horticulture,2013,37(12):103.
[4]夏光辉,刘 欢,何文兵.双酶法提取角瓜籽仁蛋白质的工艺研究[J].北方园艺,2014,38(02):137.
XIA Guang-hui,LIU Huan,HE Wen-bing.Study on Extraction Technology of Zucchini Seed Protein Using Double Enzyme Hydrolysis[J].Northern Horticulture,2014,38(12):137.
[5]张华,段倩,张可,等.化学法提取红枣渣中不溶性膳食纤维工艺研究[J].北方园艺,2013,37(14):143.
ZHANG Hua,DUAN Qian,ZHANG Ke,et al.Study on Extraction Technology of Insoluble Dietary Fiber from Jujube Slag with Chemical Method[J].Northern Horticulture,2013,37(12):143.
[6]董海丽,刘红.湿法超微粉碎提取石斛多糖的研究[J].北方园艺,2013,37(15):150.
DONG Hai-li,LIU Hong.Study on Extraction of Dendrobium candidumPolysaccharide by Wet Ultrafine Grinding Technology[J].Northern Horticulture,2013,37(12):150.
[7]高洁,黄春辉,曲雪艳,等.微波法提取猕猴桃果实中类胡萝卜素的工艺研究[J].北方园艺,2013,37(01):11.
GAO Jie,HUANG Chun-hui,QU Xue-yan,et al.Study on Extracting Conditions of Carotenoid in Kiwifruit by Microwave[J].Northern Horticulture,2013,37(12):11.
[8]王晨瑜,张雪松,王战勇,等.血红铆钉菇多糖的优化提取研究[J].北方园艺,2013,37(03):155.
WANG Chen-yu,ZHANG Xue-song,WANG Zhan-yong,et al.Study on Optimization Extraction of Polysaccharide from Gomphidius rutilus[J].Northern Horticulture,2013,37(12):155.
[9]廖春燕,黄敏,黄瑶,等.超声波辅助提取鸡骨草总皂苷的工艺研究[J].北方园艺,2013,37(03):161.
LIAO Chun-yan,HUANG Min,HUANG Yao,et al.Ultrasonic-assisted Extraction Process of Total Saponins from Abrus cantoniensis[J].Northern Horticulture,2013,37(12):161.
[10]赵广河,凌丽萍.木瓜蛋白酶法提取桃金娘多糖工艺研究[J].北方园艺,2013,37(19):131.
ZHAO Guang-he,LING Li-ping.Study on Extraction of Polysaccharides from Rhodomyrtus tomentosa with Papain Method[J].Northern Horticulture,2013,37(12):131.
[11]王玲丽,杨兆艳,郭艳茹.超声波辅助提取库拉索芦荟多糖工艺优化研究[J].北方园艺,2013,37(19):141.
WANG Ling-li,YANG Zhao-yan,GUO Yan-ru.Study on the Optimization of Extraction Techology of Polysaccharides from Aloe vera L. by Ultrasonic-assisted Method[J].Northern Horticulture,2013,37(12):141.
备注/Memo
第一作者简介：陈萍(1959-)，女，河北保定人，本科，教授，研究方向为生物科学。E-mail：shmily3205@126.com.
收稿日期：2014-01-24