ZHANG Xian-ting,LU Jing,WANG Ying-jin.Study on Optimization of Ultrasonic-assisted Extraction Technology of Polysaccharide from Zizyphus jujuba cv.Huping by Response Surface Methodology[J].Northern Horticulture,2013,37(08):150-153.
响应面法优化超声提取壶瓶枣多糖工艺研究
- Title:
- Study on Optimization of Ultrasonic-assisted Extraction Technology of Polysaccharide from Zizyphus jujuba cv.Huping by Response Surface Methodology
- 文章编号:
- 1001-0009(2013)08-0150-04
- Keywords:
- Zizyphus jujuba cv.Huping; polysaccharide; response surface methodology; process conditions
- 分类号:
- Q 946.3
- 文献标志码:
- A
- 摘要:
- 以壶瓶枣为试材，在单因素试验的基础上，选择超声温度、液料比、超声时间3个因素，利用Design-Expert 7.1.6软件Box-Benhnken中心组合试验和响应面分析法，模拟了二次多项式回归方程的预测模型，研究了各自变量交互作用对壶瓶枣多糖提取率的影响。结果表明：壶瓶枣多糖的最佳超声提取工艺为：超声温度88.0℃、液料比32.0∶1 mL/g、超声时间21 min。在此条件下，壶瓶枣多糖提取率达到(18.53±0.03)%，与理论预测值18.82%相符良好。
- Abstract:
- Taking Zizyphus jujuba cv. Huping as material,based on the experiment of single factor，the mathematical regression model was established about the dependent variable (extraction yield of polysaccharide) and independent variables (extraction temperature，ratio of liquid to solid and extraction time) through Box-Benhnken center composite design and response surface methodology，and optimization of ultrasonic-assisted extraction technology of polysaccharide from Zizyphus jujuba cv.Huping were studied.The results showed that the optimum extraction conditions were as follows：extraction temperature 88.0℃，ratio of liquid to solid 32.0∶1 mL/g，extraction time 21 min.Under these conditions，the practical yield of polysaccharide reached (18.53±0.03)%，which was consistent with the predicated yield of 18.82%.
参考文献/References:
[1]曹雁平,李菁菁,程伟,等.不同超声对姜黄色素和姜黄总黄酮浸取率影响研究[J].食品工业科技,2008,29(1):131-133. [2]樊君,吕磊,尚红伟.大枣的研究与开发进展[J].食品科学,2003,24(4):161-163. [3]王桓,潘杨,敬思群.超声强化提取喀什小枣多糖的工艺研究[J].食品研究与开发,2009,30(11):40-43. [4]郎杰,崔娜,张金良,等.酸枣果肉多糖的提取工艺和抗氧化研究[J].食品工业科技，2009,30(12):259-261. [5]李进伟,范柳萍,丁霄霖.五种枣提取物抗氧化性的比较[J].食品工业科技,2009(2):142-144. [6]Li J W，Ding S D，Ding X L.Optimization of the ultrasonically assisted extraction of polysaccharides from Zizyphus jujube cv.Jinsixiaozao[J].Journal of Food Engineering,2007,80:176-183. [7]齐慧玲,魏绍云,王继伦,等.Sevag法去除白及多糖中蛋白的研究[J].天津化工,2000(3):20-21. [8]马莺,王静,牛天骄.功能性食品活性成分测定[M].北京:化学工业出版社,2005:6-8. [9]Banik R M，Pandey S K.Selection of metal salts for alkaline phosphatase production using response surface methodology[J].Food Research International,2009,42:470-475.
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备注/Memo
第一作者简介：张先廷（1970-），男，硕士，讲师，现主要从事分析化学等研究工作。E-mail：zhangxtds@163.com.