MIN Li-jing,LI Jing-fen,ZHAO Ming-xing.Study on Optimization of Ultrasonic Assisted Extraction Technology of ?Total Flavonoids from Orange Peel[J].Northern Horticulture,2013,37(13):172-174.
超声辅助提取橘皮总黄酮的工艺优化研究
- Title:
- Study on Optimization of Ultrasonic Assisted Extraction Technology of ?Total Flavonoids from Orange Peel
- 文章编号:
- 1001-0009(2013)13-0172-03
- 分类号:
- TQ 461
- 文献标志码:
- A
- 摘要:
- 以柑橘果业加工废料橘皮为原料，以橘皮总黄酮得率为指标，通过单因素试验和正交优化，研究了超声辅助提取橘皮总黄酮的最佳工艺条件，以期为橘皮总黄酮的工业化生产提供理论指导。结果表明：超声波法提取橘皮中总黄酮的最佳提取工艺条件为：提取时间30 min，乙醇浓度60%，料液比1∶25 mg/L，此时，总黄酮的提取率可以达到96%以上。
- Abstract:
- Taking orange peel which was citrus fruit processing waste as raw material，the total flavonoids yield as index，with ultrasonic assisted extraction，through single factor experiments and orthogonal tests to optimum the extraction technology of total falvonoids from orange peel，in order to obtain optimum process conditions of orange flavonoid by ultrasonic assisted extraction and provide some theoretical guidance for the industrial production of flavonoids from orange peel.The results showed that for ultrasonic assisted extraction，the yield of orange flavonoid reached 96% under extraction conditions of extracting time 30 min，alcohol concentration 60%，solid to liquid ratio 1∶25 mg/L.
参考文献/References:
[1]范正国,章湘云.柑橘果皮综合利用的研究[J].湖南化工,2000,30(40):36-37.
相似文献/References:
[1]张 虹,王景李,白红丽,等.云南翠雀花根中总黄酮提取方法的研究[J].北方园艺,2014,38(13):153.
ZHANG Hong,WANG Jing-li,BAI Hong-li,et al.Study on the Extraction Method Total Flavonoids in Root of the Delphinium yunnanense[J].Northern Horticulture,2014,38(13):153.
[2]杨申明,王振吉,沈继森.彝药猪鬃草中总黄酮提取工艺研究[J].北方园艺,2014,38(11):125.
YANG Shen-ming,WANG Zhen-ji,SHEN Ji-sen.Study of the Extraction Technology of Total Flavonoids in Adiantum capillus-veneris[J].Northern Horticulture,2014,38(13):125.
[3]王亚红,王亚丽,祝 波.瓦松总黄酮的索氏提取工艺研究[J].北方园艺,2014,38(10):130.
WANG Ya-hong,WANG Ya-li,ZHU Bo.Study on Soxhlet Extraction Technology of Total Flavonoids From Orostachys fimbriatus[J].Northern Horticulture,2014,38(13):130.
[4]岳贤田.橘皮中天然功能因子的研究进展[J].北方园艺,2014,38(14):210.
YUE Xian-tian.Research Progress of the Natural Function Factor in the Orange Peel[J].Northern Horticulture,2014,38(13):210.
[5]韩凤波,奚广生.不同采收期对轮叶党参有效成分含量的影响[J].北方园艺,2014,38(01):154.
HAN Feng-bo,XI Guang-sheng.Effect of Different Harvest Time on the Effective Component Content of Codonopsis lanceolata [J].Northern Horticulture,2014,38(13):154.
[6]韩凤波,陈静雅.不同采收期对香椿总黄酮和总皂苷含量的影响[J].北方园艺,2014,38(02):159.
HAN Feng-bo,CHEN Jing-ya.Effect of Harvest Season on Total Saponins Content and Total Flavone Content of Toona sinensis [J].Northern Horticulture,2014,38(13):159.
[7]任吉君,王艳,肖华凤.香薷总黄酮萃取工艺参数优化研究[J].北方园艺,2013,37(14):140.
REN Ji-jun,WANG Yan,XIAO Hua-feng.Study on Optimized Extraction of Total Flavones from Elsholtzia ciliata Thunb.[J].Northern Horticulture,2013,37(13):140.
[8]王晓洁,盛东峰.不同溶剂对女贞子黄酮提取效果和抑菌活性的影响[J].北方园艺,2014,38(09):140.
WANG Xiao-jie,SHENG Dong-feng.Effect of Different Solvents on Extraction of Effective Total Flavones and Antibacterial Activity of Ligustrum lucidum [J].Northern Horticulture,2014,38(13):140.
[9]杨艳俊,王亚红,王君龙.景天三七总黄酮大孔吸附树脂纯化工艺研究[J].北方园艺,2014,38(07):144.
YANG Yan-jun,WANG Ya-hong,WANG Jun-long.Study on the Purification Process of Total Flavonoids of Sedum aizoon L. by Macroporous Adsorption Resin[J].Northern Horticulture,2014,38(13):144.
[10]朱金霞,郑国保,孔德杰,等.甘草中甘草苷、甘草酸及总黄酮的测定及其含量相关性研究[J].北方园艺,2014,38(03):149.
ZHU Jin-xia,ZHENG Guo-bao,KONG De-jie,et al.Study on the Determination of Liquiritin,Glycyrrhizic Acid and Total Flavonoids in Licoric and Their Relationships[J].Northern Horticulture,2014,38(13):149.
备注/Memo
第一作者简介：闵莉静（1981-），女，硕士，实验师，研究方向为天然产物的提取和纯化及结构修饰。E-mail:minlijing1981@163.com.