LI Li,LI Ling,YU Xia,et al.Study on Extraction of Total Flavonoids From the Root of Jasminum duclouxii by Microwave-Assisted Route[J].Northern Horticulture,2015,39(15):124-127.[doi:10.11937/bfyy.201515033]
微波辅助云南鸡爪花根总黄酮提取工艺研究
- Title:
- Study on Extraction of Total Flavonoids From the Root of Jasminum duclouxii by Microwave-Assisted Route
- Keywords:
- microwave; root of Jasminum duclouxii; total flavonoids
- 文献标志码:
- A
- 摘要:
- 以云南鸡爪花根为原料，乙醇溶液为提取剂，采用单因素试验和正交实验相结合方法，研究了料液比、乙醇浓度、微波加热时间及微波加热功率等工艺参数对总黄酮得率的影响。结果表明：鸡爪花根总黄酮的最佳提取工艺为料液比1∶20 g/mL，乙醇浓度50%，提取时间60 s，微波功率350 W，总黄酮平均得率为2.21%。利用微波辅助法提取鸡爪花根总黄酮类物质，具有简单实用的特点，可大大缩短提取时间，达到省时、节能和高效的目的。
- Abstract:
- Taking Jasminum duclouxii as test materials，the technology of extraction of the total flavonoids from the root of Jasminum duclouxii was studied to provide a reference for it’s further study and utilization，taking the root of Jasminum duclouxii as material，and alcohol as extractant，the effect of solid-1iquid ratio，ethanol concentration，extracting time and microwave power on the extraction of the total flavonoids from the root of Jasminum duclouxii was investigated using the methods of single factor test and orthogonal design test of L9(34).The results showed that the highest extraction rate (2.21%) of the total flavonoids in the root of Jasminum duclouxii could be obtained under conditions of solid-1iquid ratio 1∶20 g/mL，50% ethanol，extracting time 60 seconds，microwave power 350 W.The microwave-assisted extraction of flavonoids from Jasminum duclouxii was simple and practical，which was time saving，energy conserving and high efficient.
参考文献/References:
[1]赵桂琴,毛晓霞,苏占辉.素馨花中黄酮苷类化学成分研究[J].中国新药杂志,2012,21(7):791-794. [2]刘成海,游海.天然产物有效成分的分离与应用[M].北京:化学工业出版社,2002. [3]李楠,刘元,侯滨滨,等.黄酮类化合物的功能特性[J].食品研究与开发,2005,26(6):139-141. [4]赵象忠.天梯山人参果黄酮有机溶剂提取工艺的研究[J].中国食物与营养,2014,20(3):47-51. [5]刘金香,王水兴,范青生.碱溶酸沉法提取银杏叶总黄酮[J].安徽农业科学,2008,36(26)：11386-11388. [6]易建华,朱振宝.响应面优化酶法提取芹菜黄酮工艺研究[J].食品科学,2009,30(10):92-96. [7]高荫榆,游海,陈芩,等.蜂胶黄酮类化合物超临界萃取工艺研究[J].食品科学,2002,23(8):154-157. [8]王丽霞,刘坤.超声波辅助提取玉米须黄酮工艺[J].北方园艺,2014(6):137-139. [9]陈伟,刘青梅,杨性民,等.微波技术在杜仲黄酮提取工艺中的应用研究[J].食品科学,2006，27(10):285-288. [10]史高峰,邓丽,李永红,等.微波辅助混合溶剂提取甘草渣中总黄酮的工艺[J].食品研究与开发,2011,10(32):42-45. [11]周达,罗成,鲁晓翔,等.玫瑰花总黄酮微波辅助提取及抗氧化性研究[J].食品工业科技,2010,4(4):269. [12]韩忠明,刘翠晶,胡顺波.中华苦荬菜总黄酮微波提取工艺研究[J].北方园艺,2011(24):207-210. [13]龚磊,黄小容,龚其海,等.微波辅助提取瑞香狼毒总黄酮工艺条件的优化[J].郑州大学学报(医学版),2013,48(2):242-244.
相似文献/References:
[1]许 建,廖 亮,再吐娜·买买提,等.间歇式低温微波处理对哈密瓜汁品质及过氧化物酶活性的影响[J].北方园艺,2014,38(08):119.
XU Jian,LIAO Liang,ZAITUNA·Maimaiti,et al.Effect of Intermittent Low Temperature Microwave on Quality and POD Activity of Hami Melon Juice[J].Northern Horticulture,2014,38(15):119.
[2]胡志辉,张繁荣,周世力,等.CTP-3和微波处理对食用菌栽培基质三种常见杂菌的灭菌效果研究[J].北方园艺,2014,38(08):135.
HU Zhi-hui,ZHANG Fan-rong,ZHOU Shi-li,et al.Disinfection Test on Three Kinds of Bacterium in the Edible Fungi Treated With CTP-3 and Microwave[J].Northern Horticulture,2014,38(15):135.
[3]徐东生.微波提取山药黄酮的方法研究[J].北方园艺,2014,38(15):139.
XU Dong-sheng.Study on Extraction Total Flavonoids by Microwave From Dioscorea opposita[J].Northern Horticulture,2014,38(15):139.
[4]徐东生.微波提取黄芪黄酮的方法研究[J].北方园艺,2015,39(03):113.[doi:10.11937/bfyy.201503033]
XU Dong-sheng.Study on Extraction Total Flavonoids by Microwave from Astragalus membranaceus[J].Northern Horticulture,2015,39(15):113.[doi:10.11937/bfyy.201503033]
[5]吴中军,夏晶晖,吴 夏.复合保鲜技术对马蹄莲切花保鲜效果的影响[J].北方园艺,2015,39(23):142.[doi:10.11937/bfyy.201523040]
WU Zhongjun,XIA Jinghui,WU Xia.Effect of Compound Preservation Technology on Fresh Keeping of Cut Calla Lily[J].Northern Horticulture,2015,39(15):142.[doi:10.11937/bfyy.201523040]
[6]孙海涛,邵信儒,姜瑞平,等.超声波-微波联合提取山核桃壳多酚及其稳定性[J].北方园艺,2015,39(24):135.[doi:10.11937/bfyy.201524037]
SUN Haitao,SHAO Xinru,JIANG Ruiping,et al.Study on Ultrasound-Microwave Combined Extraction and Stability of Pecan Shell Polyphenolic[J].Northern Horticulture,2015,39(15):135.[doi:10.11937/bfyy.201524037]
[7]孙海涛,孙影,朱炎,等.超声波-微波协同酶法提取柳蒿芽黄酮[J].北方园艺,2016,40(05):153.[doi:10.11937/bfyy.201605040]
SUN Haitao,SUN Ying,ZHU Yan,et al.Optimization of Flavonoids Extraction Technology From Artemisia integrifolia L.by Ultrasound-microwave Enzyme Synergistic Method[J].Northern Horticulture,2016,40(15):153.[doi:10.11937/bfyy.201605040]
[8]张水花,江永刚,赵红艳.多汁乳菇多糖的微波辅助提取工艺及其清除DPPH自由基研究[J].北方园艺,2016,40(14):135.[doi:10.11937/bfyy.201614034]
ZHANG Shuihua,JIANG Yonggang,ZHAO Hongyan.Microwave-assisted Extraction and Antioxidant Activity of Polysaccharides From Lactarius volemus Fr.[J].Northern Horticulture,2016,40(15):135.[doi:10.11937/bfyy.201614034]
[9]张水花,李本鸿.微波辅助提取油黄口蘑多糖工艺及其体外抗氧化性研究[J].北方园艺,2018,42(20):120.[doi:10.11937/bfyy.20180052]
ZHANGShuihua,LIBenhong.Microwave-assistedExtractionandAntioxidantActivityof PolysaccharidesFromTricholomaflavovirensLundell[J].Northern Horticulture,2018,42(15):120.[doi:10.11937/bfyy.20180052]
[10]朱香澔,段振华,刘艳,等.食用菌菌棒微波灭菌工艺优化[J].北方园艺,2018,42(23):143.[doi:10.11937/bfyy.20180902]
ZHU Xianghao,DUAN Zhenhua,LIU Yan,et al.Optimization of Microwave Sterilization Process of Edible Fungus Culture Rods[J].Northern Horticulture,2018,42(15):143.[doi:10.11937/bfyy.20180902]
备注/Memo
第一作者简介：李丽（1982-），女，云南昌宁人，硕士，讲师，研究方向为催化化学。E-mail：lili19820607@126.com. 基金项目：保山学院科研教研基金重点资助项目（13BZ012）。