CAI Yan,WANG Kefeng,DONG Ran,et al.Components of Volatile Oil From Allium victorialis L.[J].Northern Horticulture,2017,41(21):140-145.[doi:10.11937/bfyy.20170891]
长白山茗葱挥发油成分分析
- Title:
- Components of Volatile Oil From Allium victorialis L.
- 文献标志码:
- A
- 摘要:
- 以长白山茗葱为试材,采用顶空固相微萃取法对其不同部位的挥发油进行提取,通过GC-MS联用技术进行分析鉴定,利用峰面积归一化法计算各化合物的相对质量分数。结果表明:从茗葱根挥发油中得到37个色谱峰,共鉴定出33种化合物,其中2,3-去氢-1,8-桉叶素(50.616%)、甲基-2-烯丙基二硫醚(19.036%)质量分数相对较高;鳞茎挥发油中得到21个色谱峰,共鉴定出19种化合物,其中硫化丙烯(28.459%)、二烯丙基二硫(27.765%)质量分数较高;叶片挥发油中得到24个色谱峰,共鉴定出22种化合物,其中(Z)乙酸叶醇酯(55.910%)、乙酸反-2-己烯酯(9.183%)2种化合物质量分数较高。HS-SPME GC-MS是一种可用于分析不同部位茗葱挥发油成分变化的简单可行的分析方法。
- Abstract:
- Taking Allium victorialis L.as test material,the volatile oils extracted from the Allium victorialis L.by HS-solid-phase microextraction(SPME) were studied.Chemical constituents were identified by GC-MS.The compound quantification was calculated using the area normalization method.The results showed that 37 chromatographic peaks separated well were found in the roots of the volatile oils;33 compounds were identified in the oils of roots of Allium victorialis L.,including 2,3-Dehydro-1,8-cineole (50.616%),Disulfide,methyl 2-propenyl(19.036%).From the volatile oils of bulbs,21 chromatographic peaks separated well were found in the respective GC total ion current chromatograms of oils.19 compounds were identified in the oils of bulbs in cluding Thiirane,methyl(28.459%),Diallyl disulphide (27.765%);24 chromatographic peaks separated well were found in the respective GC total ion current chromatograms of oils;22 compounds were identified in the oils of lesves of Allium victorialis L.3-Hexen-1-ol,acetate, (Z)-(55.910%) 2-Hexen-1-ol,acetate,(E)-(9.183%) were the main components.Headspace SPME-GC-MS is a simple sampling method for measuring the variations of main constituents in volatile fragrance from fresh Allium victorialis L.
参考文献/References:
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备注/Memo
第一作者简介:才燕(1982-),女,硕士,讲师,研究方向为长白山特色植物资源开发与利用。E-mail:10058218@qq.com.