[1]王斌,王凤君,梁颖琪,等.玫瑰纯露提取工艺优化及其抑菌和抗氧化活性研究[J].北方园艺,2020,44(18):106-113.[doi:10.11937/bfyy.20194233]
　WANG Bin,WANG Fengjun,LIANG Yingqi,et al.Study on Extraction Process Optimization of Rose Hydrosol and Its Antibacterial and Antioxidant Activities[J].Northern Horticulture,2020,44(18):106-113.[doi:10.11937/bfyy.20194233]
点击复制

玫瑰纯露提取工艺优化及其抑菌和抗氧化活性研究

《北方园艺》[ISSN:1001-0009/CN:23-1247/S] 卷: 第44卷 期数: 2020年18 页码: 106-113 栏目: 出版日期: 2020-09-30
Title:
Study on Extraction Process Optimization of Rose Hydrosol and Its Antibacterial and Antioxidant Activities
作者:
王斌1; 王凤君1; 梁颖琪1; 王德琪2; 何金明1
（1.韶关学院 英东生物与农业学院/韶关市芳香植物工程技术研究中心,广东 韶关 512005；2.广东华拓生物科技有限公司,广东 韶关 512600）
Author(s):
WANG Bin1; WANG Fengjun1; LIANG Yingqi1; WANG Deqi2; HE Jinming1
(1.Henry Fok College of Biology and Agriculture/Shaoguan Aromatic Plant Engineering Technology Research Center,Shaoguan University,Shaoguan,Guangdong 512005;2.Guangdong Huatuo Biotechnology Limited Company,Shaoguan,Guangdong 512600)
关键词:
玫瑰纯露; 工艺优化; 响应面法; 抑菌活性; 抗氧化活性
Keywords:
rose hydrosol; process optimization; response surface methodology; antibacterial activity; antioxidative activity
DOI:
10.11937/bfyy.20194233
文献标志码:
A
摘要:
以“中天”玫瑰花朵为试材，采用水蒸气蒸馏法提取玫瑰纯露，通过响应面试验优化了玫瑰纯露的提取工艺，并评价了玫瑰纯露的抑菌和抗氧化活性，以期为玫瑰纯露的开发利用提供参考依据。结果表明：在花液比为1∶1.7 g?mL-1、回流时间为7 min、蒸馏温度为120 ℃的条件下，获得的纯露感官评分最高；在该条件下提取的玫瑰纯露对DPPH?和超氧阴离子的清除率分别为24.66%和5.03%，对微生物生长具有明显抑制作用，表明提取的玫瑰纯露具有较好的抑菌和抗氧化活性。
Abstract:
Taking rose ‘Zhongtian’ petals as materials,hydrosols were extracted by using the method of steam distillation.The extraction process of rose hydrosol was optimized by response surface methodology,and antibacterial and antioxidant activities of rose hydrosol were evaluated,in order to provide basis for the development and utilization of rose hydrosol.The results showed that under the condition of flower-liquid ratio of 1∶1.7 g?mL-1,reflux time of 7 minutes and distillation temperature at 120 ℃,the obtained hydrosol showed the highest sensory score.Under this condition,the scavenging rate of rose hydrosol against DPPH? and superoxide anion were 24.66% and 5.03%,respectively,and which could obviously inhibit the growth of microorganisms,suggesting that the extracted rose hydrosol had strongly antibacterial and antioxidative activities.

参考文献/References:

[1]徐宗大,赵兰勇,张玲,等.玫瑰SRAP遗传多样性分析与品种指纹图谱构[J].中国农业科学,2011,44(8):1662-1669.[2]王再花,容静东,王玉丰,等.‘中天’玫瑰在广东怀集引种栽培及花朵营养成分分析[J].广东农业科学,2018,45(11):28-34.[3]李俊芳,常乐.玉米玫瑰复合型酸奶的制备工艺研究[J].广东农业科学,2011,38(21):103-105.[4]古娜斯?叶尔肯,冯作山,等.响应面法优化玫瑰花酱无硫护色剂配方[J].食品工业,2017,38(9):42-47.[5]饶建平,王文成,张远志,等.水蒸气蒸馏法提取柚子花精油工艺研究及其成分分析[J].食品工业科技,2017,38(4):236-240.[6]李娟娟,王羽梅,潘春香,等.不同氮素形态及配比对薄荷精油含量和品质的影响[J].植物生理学报,2016,52(2):150-156.[7]LEI G,ZHANG A,LIU X,et al.Study on the recovered essential oil obtained from hydrosol of Yulania denudata fresh flowers[J].Journal of Essential Oil Research,2015,27(2):153-159.[8]李天越.桔皮精油提取和综合利用探究[J].石化技术,2019,26(3):94-95.[9]TAJKARIMI M M,IBRAHIM S A,CLIVER D O.Antimicrobial herb and spice compounds in food[J].Food Control,2010,21:1199-1218.[10]BURT S.Essential oils：Their antibacterial properties and potential applications in foods-a review[J].International Journal of Food Microbiology,2004,94:223-253.[11]杨正青,薛文昊,苗延青.玫瑰精油的提取及抑菌活性研究[J].广东化工,2019,46(5):28-29.[12]王珍,郑霞,周琛彦,等.月季花纯露提取的最佳工艺及有效成分的验证[J].连云港师范高等专科学校学报,2017,34(4):108-113.[13]李向波,刘顺航,贾黎晖,等.普洱茶感官品质分析及风味轮构建[J].中国茶叶,2017,39(11):32-34.[14]张作法.桑枝活性成分分离纯化及其药理作用的研究[D].杭州:浙江大学,2008.[15]孟慧,刘洋洋,杨云.四种芳香植物纯露体外抗氧化活性研究[J].化学与生物工程,2014,31(6):22-24.[16]鹿浩志,刘敏轩,田亚亚,等.生姜精油的提取及GC-MS分析[J].食品工业科技,2019,40(14):208-213.[17]廖瑟静,翁竞玉,石榆锋,等.桧木纯露解酒护肝作用的实验研究[J].食品研究与开发,2019,40(8):184-187.[18]张乐宏,刘静,邓阳,等.梧桐籽抗氧化活性成分提取工艺的优化[J].青岛农业大学学报(自然科学版),2019,36(3):192-199.[19]白雨鑫.萝摩果壳多糖提取工艺优化及药理活性的研究[D].锦州:锦州医科大学,2016.[20]DOROSHOW J H,DAVIES K J.Redox cycling of anthracyclines by cardiac mitochondria.II.Formation of superoxide anion,hydrogen peroxide,and hydroxyl radical[J].Journal of Biological Chemistry,1986,261(7):3068-3074.[21]牟真靓,陈灿杨,邹心茹,等.薄荷纯露对黄瓜种子发芽及幼苗生长的影响[J].韶关学院学报,2019,40(12):61-66.[22]李珍,哈益明,李安,等.响应面优化苹果皮渣多酚超声提取工艺研究[J].中国农业科学,2013,46(21):4569-4577.[23]任洪涛,周斌.香叶天竺葵精油和纯露的挥发性成分分析及抗氧化活性评价[J].日用化学工业,2017,47(8):463-467.[24]梁卉,刘绍华,欧阳坚,等.5种芳香中药纯露体外抗氧化活性及抑菌活性分析[J].香料香精化妆品,2018(3):58-60.[25]付春雪.黑龙江罗马洋甘菊挥发油和纯露成分分析及抑菌实验研究[D].佳木斯:佳木斯大学,2019.

相似文献/References:

[1]刘细祥,张婷婷,卢芳泉,等.响应面法优化香蕉皮中单宁提取工艺研究[J].北方园艺,2014,38(08):125.
　LIU Xi-xiang,ZHANG Ting-ting,LU Fang-quan,et al.Optimization of Extraction Process for Tanin From Banana Peel by Response Surface Methodology[J].Northern Horticulture,2014,38(18):125.
[2]焦 镭,柴梦颖,石明生,等.碱性条件下山楂叶总黄酮的提取工艺研究[J].北方园艺,2014,38(08):128.
　JIAO Lei,CHAI Meng-ying,SHI Ming-sheng,et al.Study on the Extraction Technology of Total Flavonoids From Hawthorn Leaf in Alkaline Conditions[J].Northern Horticulture,2014,38(18):128.
[3]吴恒梅,李春丰,姜成,等.中药饮片中丝瓜络碱溶性多糖提取工艺的优化[J].北方园艺,2014,38(07):124.
　WU Heng-mei,LI Chun-feng,JIANG Cheng,et al.Extraction Process Optimization of Loofah Alkali Soluble Polysaccharide in the Chinese Medicine Decoction Pieces[J].Northern Horticulture,2014,38(18):124.
[4]王为兰,陈开旭,马纪,等.新疆阿魏菇的干燥工艺优化及活性成分初步鉴定[J].北方园艺,2016,40(04):137.[doi:10.11937/bfyy.201604035]
　WANG Weilan,CHEN Kaixu,MA Ji,et al.Optimization of Drying Process and Characterization of Active Components of Pleurotus ferulae[J].Northern Horticulture,2016,40(18):137.[doi:10.11937/bfyy.201604035]
[5]李成华,薛长松,李丽.酸浆宿萼总黄酮提取工艺优化及其抗氧化活性[J].北方园艺,2018,42(23):124.[doi:10.11937/bfyy.20180722]
　LI Chenghua,XUE Changsong,LI Li.Optimized Extraction and Antioxidant Activity of Flavonoid From Physali alkekengi L.[J].Northern Horticulture,2018,42(18):124.[doi:10.11937/bfyy.20180722]
[6]贾洪信,周喜华,刘素纯.基于模糊数学综合评价法优化平菇肉松制作工艺[J].北方园艺,2018,42(24):118.[doi:10.11937/bfyy.20180895]
　JIA Hongxin,ZHOU Xihua,LIU Suchun.Optimization of Dried Pleurotus ostreatus Meat Floss Processing Based on Fuzzy Mathematic Evaluation[J].Northern Horticulture,2018,42(18):118.[doi:10.11937/bfyy.20180895]
[7]薛山,刘泽明.鹰嘴芒皮渣水不溶性膳食纤维提取工艺优化及理化性质测定[J].北方园艺,2019,43(07):114.[doi:10.11937/bfyy.20182665]
　XUE Shan,LIU Zeming.Optimization of Extraction Process and Determination of Physicochemical Properties of Water Insoluble Dietary Fiber From Golek Peel[J].Northern Horticulture,2019,43(18):114.[doi:10.11937/bfyy.20182665]
[8]李荣峰,许彩勤.金线莲黄酮类化合物的提取工艺[J].北方园艺,2020,44(11):98.[doi:10.11937/bfyy.20193275]
　LI Rongfeng,XU Caiqin.Extraction Technology of Flavonoids Compounds From Anoectochilus[J].Northern Horticulture,2020,44(18):98.[doi:10.11937/bfyy.20193275]
[9]武洪敏,高青青,陈庚,等.双水相法萃取白及多糖及其对亚硝酸盐的清除作用[J].北方园艺,2021,(03):114.[doi:10.11937/bfyy.20201469]
　WU Hongmin,GAO Qingqing,CHEN Geng,et al.Extraction Polysaccharides From Bletilla striata by Aqueous Two Phase System and Its Clearance to Nitrite[J].Northern Horticulture,2021,(18):114.[doi:10.11937/bfyy.20201469]
[10]郁万文,杨森,赵丹,等.响应面优化超声辅助乙醇提取银杏叶莽草酸工艺[J].北方园艺,2024,(19):99.[doi:10.11937/bfyy.20241071]
　YU Wanwen,YANG Sen,ZHAO Dan,et al.Response Surface Optimization of Ultrasound-assisted Ethanol Extraction of Shikimic Acid From Ginkgo biloba Leaves[J].Northern Horticulture,2024,(18):99.[doi:10.11937/bfyy.20241071]

备注/Memo

第一作者简介：王斌（1991-），男，甘肃秦安人，博士，讲师，现主要从事农产品加工及贮藏工程等研究工作。E-mail：b_wangsgu@163.com.责任作者：何金明(1973-)，男，满族，内蒙古通辽人，博士，教授，现主要从事芳香植物资源开发与利用等研究工作。E-mail：jmh-3183@163.com.基金项目：韶关市科技计划资助项目（2019sn085）；韶关学院校级重点资助项目（SZ2018KJ02）；韶关学院大学生创新创业训练计划资助项目（Sycxcy2019084）。收稿日期：2019-11-08

更新日期/Last Update: 2020-12-23