ZHENG Tao,SU Rui,ZHAO Yun-mei,et al.Optimization of Ultrasonic Extraction of Polyphenols from the Leaves of Picea wilsonii[J].Northern Horticulture,2013,37(22):138-140.
青杄针叶多酚超声提取工艺的优化
- Title:
- Optimization of Ultrasonic Extraction of Polyphenols from the Leaves of Picea wilsonii
- 文章编号:
- 1001-0009(2013)22-0138-03
- Keywords:
- Picea wilsonii; polyphenols; extraction; orthogonal test
- 分类号:
- S 791. 18
- 文献标志码:
- A
- 摘要:
- 以青杄针叶为试材，以乙醇为提取剂，采用超声提取法，通过正交实验研究优化了青杄针叶总多酚的最佳提取工艺。结果表明：影响青杄针叶中总多酚提取的因素大小依次为：料液比>超声功率>超声温度>超声时间，最优的提取工艺是料液比1∶60 g/mL，超声功率为350 W，超声温度为45℃，超声时间35 min，在此条件下，多酚提取率为34.72%。
- Abstract:
- Taking the leaves of Picea wilsonii as material,ethanol as extraction solvent,adopting ultrasonic extraction method,the extraction of polyphenols was investigated by orthogonal test method.The results showed that the influence factors on the extraction rate of polyphenols was the order of material liquid ratio>ultrasonic power>ultrasonic temperature>ultrasonic time,and the optimum condition was material liquid ratio 1∶60 g/mL,ultrasonic power 350 W,ultrasonic temperature 45℃,ultrasonic time 35 min,under the condition,the polyphenols extraction rate was 34.72%.
参考文献/References:
[1] 陈思,董永恒,高智辉,等.甘肃兴隆山保护区青杄群落结构分析[J].西北林学院学报,2013(1):39-45.
[2] Kimy S,Shin D H.Volatile components and antibacterial effects of pine needle(Pinus densiflora S.and Z.)extract[J].Food Microbiology,2005(22):37-45.
[3] Su X Y,Wang Z Y,Liu J R.In vitro and in vivo antioxidant activity of Pinus koraiensis seed extract containing phenolic compounds[J].Food Chemistry,2009,117(4):681-686.
[4] 曹炜,索志荣.Folin-Ciocalteu比色法测定蜂蜜中总酚酸的含量[J].食品与发酵工业,2003(12):80-82.
[5] 房祥军,郜海燕,陈杭君.正交试验法优化山核桃仁中总多酚的提取工艺参数研究[J].中国食品学报,2009(1):153-157.
[6] 贾冬英,姚开,谭薇,等.石榴皮中多酚提取条件的优化[J].林产化学与工业,2006(3):123-126.
[7] 李光,余霜,陈庆富.正交设计在红薯叶黄酮提取中的应用[J].北方园艺,2012(1):41-42.
[8] 孙海燕,郭伟.正交实验优选向日葵叶片提取总黄酮的研究[J].北方园艺,2013(3):16-18.
[9] 石碧,狄莹.植物多酚[M].北京:科学出版社,2000.
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备注/Memo
第一作者简介：郑涛（1989-），男，硕士研究生，研究方向为植物资源利用。E-mail:zhenghaust@163.com.
责任作者：樊金拴（1958-），男，教授，博士生导师，研究方向为植物资源利用。E-mail:fanjinshuan@163.com.
收稿日期：2013-06-24