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Optimization and Component Analysis of Ultrasonic-microwave Synergistic Extraction of Organic Sulfur-containing Compounds From Allium cepa L.var.agrogatum Don

《北方园艺》[ISSN:1001-0009/CN:23-1247/S]

Issue:
2021年04
Page:
93-100
Research Field:
Publishing date:

Info

Title:
Optimization and Component Analysis of Ultrasonic-microwave Synergistic Extraction of Organic Sulfur-containing Compounds From Allium cepa L.var.agrogatum Don
Author(s):
ZHANG Yanling1QIN Yuting2ZHAO Wenting23LIU Hongcheng24LIU Tingting25
(1.Jilin Engineering Normal University,Changchun,Jilin 130052;2.College of Food Science and Engineering,Jilin Agricultural University,Changchun,Jilin 130118;3.Key Laboratory of Technological Innovations for Grain Deep-processing and High-effeciency Utilization of By-products of Jilin Province,Changchun,Jilin 130118;4.Engineering Research Center of Grain Deep-processing and High-effeciency Utilization of Jilin Province,Changchun,Jilin 130118;5...
Keywords:
ultrasonic-microwave synergistic extractionAllium cepa L.var.agrogatum Donorganic sulfur-containing compoundsgas chromatography-mass spectrometry
PACS:
-
DOI:
10.11937/bfyy.20200566
Abstract:
Taking Allium cepa L.var.agrogatum Don as test material,organic sulfur-containing compounds were extracted by ultrasonic-microwave synergistic extraction.The process optimization test of organic sulfur compounds were carried out,and the components of extraction were separated and identified by gas chromatography-mass spectrometry in order to provide a reference for further research and development of functional components of Allium cepa L.var.agrogatum Don.The results showed that the optimal extraction process was the microwave temperature of 55 ℃,the ratio of material-liquid of 1∶8 g?mL-1,the synergistic time of 6 minutes,the stirring speed of 300 r?min-1,and the ultrasonic power of 500 W.The yield of the organic sulfur-containing compounds obtained under the above conditions was 0.277 1%±0.002 3%.Under this condition,fifteen kinds of organic sulfur-containing compounds were obtained.The higher content was thiophenes 39.067 8%±0.004 3%,followed by trisulfide compounds 14.157 0%±0.007 1% and thioethers 7.387 2%±0.005 2%.Among them,the relatively high content of organic sulfur-containing compounds was 2,4-dimethyl-thiophene,3,5-diethyl-1,2,4-trithiolane,diallyl disulphide.

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Last Update: 2021-06-07