|Table of Contents|

Method Optimization of Determing of Soil Available Phosphorus With  Continuous Flow Analytical System

《北方园艺》[ISSN:1001-0009/CN:23-1247/S]

Issue:
2018年07
Page:
94-98
Research Field:
Publishing date:

Info

Title:
Method Optimization of Determing of Soil Available Phosphorus With  Continuous Flow Analytical System
Author(s):
PANG Shihua12SHEN Yanhui1YANG Yuanguang1SUN Defang1CHEN Hongkun12
(1.Kingenta Ecological Engineering Group Co.Ltd.,Linshu,Shandong 276700;2.State Key Laboratory of Nutrition Resources Integrated Utilization, Linshu,Shandong 276700)
Keywords:
continuous flow analyzer (CFA)molybdenum antimony colorimetric methodoptimizedefinition
PACS:
-
DOI:
10.11937/bfyy.20173182
Abstract:
Acidic, neutral and alkaline soil were used as research object and tested available P content by continuous flow analyzer(CFA)under the condition of reducing surfactant and increasing detecting efficiency, and evaluated the method accuracy to test leaching liquor of available P.The results showed that there was no significant difference of the soil available P contents measured by CFA and ultraviolet spectrophotometry method.A linear equation could best describe their relationship,Y (CFA-P)=1.103 5X (ultraviolet spectrophotometer-P)-6.439 7.The pearson′s correlation coefficient was 0.999 with a significance level (n=61,P<0.01).The CFA method for soil available P measurement had high precision with relative standard deviation (RSD) less than 1.2%.In summary, after reducing surfactant and improving detection efficiency, continuous flow analyzer could detect soil available phosphorus faster, lower cost, better repeatability, and could meet the requirements of detection.

References:

 

[1]夏倩,刘凌,王流通,等.连续流动分析仪在水质分析中的应用[J].分析仪器,2012(2):64-68.

[2]ESTELA J M,CEND V.Flow analysis techniques for phosphorus:An overview[J].Talanta,2005,66(2):307-331.

[3]MCLEOD S.Determination of total soil and plant nitrogen using a micro-distillation unit in a continuous flow analyzer[J].Anal Chim Acta,1992,266:113-117.

[4]张英利,许安民,尚浩博,等.连续流动分析仪测定土壤硝态氮和有效磷的试验及改进[J].中国土壤与肥料,2008(2):77-80.

[5]张英利,尚浩博,马爱生,等.连续流动注射法测定土壤和植株中全磷[J].理化检测(化学分册),2007,43(8):649-652.

[6]鲍士旦.土壤农化分析[M].3版.北京:中国农业出版社,2000:79-83.

[7]王斗文,施昌彦,曹实,等.检测实验室中常用不确定度评定方法与表示:GB/T 27411-2012[S].北京:中华人民共和国国家质量监督检验检疫总局,2012.

[8]叶德培,赵峰,施昌彦,等.测量不确定度评定与表示:JJF1059.1-2012[S].北京:国家质量监督检验检疫总局,2012.

[9]马长宝,郑磊,辛景树,等.土壤有效磷的测定连续流动分析仪法:NY/T 1121.25-2012[S].济南:山东省标准化研究院,2012.

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Last Update: 2018-04-20