|Table of Contents|

Study on Technology of Static Purification of Lignans from Schisandra chinensis Baill by Macroporous Adsorption Resin(PDF)

《北方园艺》[ISSN:1001-0009/CN:23-1247/S]

Issue:
2015年07
Page:
141-145
Research Field:
Publishing date:

Info

Title:
Study on Technology of Static Purification of Lignans from Schisandra chinensis Baill by Macroporous Adsorption Resin
Author(s):
CHENG Zhen-yu1; SONG Hai-yan2; YANG Ying-jie1; XUE Jun-li1; JI Hui-jie1
（1.College of Chemical and Pharmaceutical Engineering，Jilin Institute of Chemical Technology，Jilin，Jilin 132022；2.Center of Experiments，Jilin Agricultural Science and Technology College，Jilin，Jilin 132101）
Keywords:
high performance liquid chromatography; Schisandra chinensis Baill; lignans; macroporous adsorption resin; purification
PACS:
-
DOI:
10.11937/bfyy.201507041
Abstract:
Taking Schisandrol A，Schisantherin A，Deoxyschisandrin，Schisandrin B and Schisandrin C as test index，the static purification conditions of lignans were determined on the basis of investigating the adsorption and desorption performance of different kind of macroporous resins.The results showed that,AB-8 macroporous resins was chose and employed in this study，the optimal adsorption conditions were as follows：adsorption sample volumes of 40 mL，pH value of 6.6，adsorption temperature of 55℃ and adsorption time of 10 hours；the optimal desorption conditions were desorption time of 8 hours，desorption temperature of 65℃，dehydrated ethanol as desorption solvent and the volume of 150 mL.Under these optimal conditions，the lignans content of Schisandra crude extracts increased from 0.98% to 5.86%.The method proposed in this study provided data and theoretical support.

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Last Update: 2015-07-24