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Study on Extraction Process and Content of Salicylic Acid from Rubus cratacgifolius(PDF)

《北方园艺》[ISSN:1001-0009/CN:23-1247/S]

Issue:
2014年16期
Page:
127-130
Research Field:
Publishing date:

Info

Title:
Study on Extraction Process and Content of Salicylic Acid from Rubus cratacgifolius
Author(s):
ZHAO Wei-weiLI Ai-minZHANG Zheng-haiZHANG YueCHEN Xiao-dan
Institute of Specialty,Chinese Academy of Agricultural Sciences,Changchun,Jilin 130112
Keywords:
Rubus cratacgifoliussalicylic acidextraction process
PACS:
S663.2
DOI:
-
Abstract:
Taking Rubus cratacgifolius as material,the extraction conditions of the free and bound salicylic acid in Rubus cratacgifolius were optimized by orthogonal test.The results showed that the best extraction conditions for free salicylic acid were:acetonitrile as the extraction solvent and adding phosphate,ultrasound 15 min;for bound salicylic acid were diehyl ether as the extraction solvent and adding phosphate,ultrasound 15 min.The free and bound salicylic acid displayed similar trends in Rubus cratacgifolius shoots or fruits (r=0.868**and 0.986**);the salicylic acid content of new shoots shown a higher levels (1.179 mg/g) before flowering,and declined gradually from flowering period to fruit development period (Chinese white olive period),increased gradually from coloring to fully mature period,and a sharp rise after picking the fruit in mid-August (1.434 mg/g).In a word,the salicylic acid content of fruit decreased in the whole growth period,and showed higher level than mature period.

References:

[1]Paterson J,Baxter G,Lawrence J,et al.Is there a role for dietary salicylates in health[J].Proceedings of the Nutrition Society,2006,65:93-96.

[2]Dini P V,Peter C H,Hollman J,et al.Determination of acetylsalicylic acid and salicylic acid in foods,using HPLC with fluorescence detection[J].J Agric Food Chem,1996,44(7):1762-1767.
[3]徐幼平,马志超,蔡新忠.反相高效液相色谱测定番茄组织中的水杨酸[J].植物生理学通讯,1997(1):49-52.
[4]李兆亮,原永兵,李冬梅.薄层层析和高效液相层析技术结合测定植物叶片水杨酸含量[J].植物生理学通讯,1997(2):130-132.
[5]张玉,陈昆松,张上隆.猕猴桃果实中内源水杨酸的提取测定及其在采后研究中的应用[J].中国食品学报,2004,4(3):6-9.
[6]邓文红,张风娟,金幼菊.反相高效液相色谱法测定植物组织中的水杨酸[J].北京林业大学学报,2007(1):151-154.
[7]薛峰,林毅侃,马跃龙,等.食品中水杨酸含量测定方法的研究进展[J].食品工业科技,2012(14):429-431.
[8]Swain A R,Dutton S P,Truswell A S,et al.Salicylates in food [J].Nutrition Reviews,1996,54:357-359.
[9]Michael J S,Dominic P T R,Lesley A W,et al.Free salicylic acid and acetyl salicylic acid content of foods using gas chromatography-mass spectrometry[J].Food Chemistry,2007,105:273-279.

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Last Update: 2014-09-26