|Table of Contents|

Study on the Extraction Technology of Total Saponins from Hovenia dulcis(PDF)

《北方园艺》[ISSN:1001-0009/CN:23-1247/S]

Issue:
2013年20期
Page:
129-130
Research Field:
Publishing date:

Info

Title:
Study on the Extraction Technology of Total Saponins from Hovenia dulcis
Author(s):
LAN GuangLI YangSUN Jia-li
College of Food Engineering,Jilin Agricultural Science and Technology College,Jilin,Jilin 132101
Keywords:
Hovenia dulcistotal saponinsextraction technology
PACS:
TS 255.36
DOI:
-
Abstract:
Taking Hovenia dulcis as material,using acid-base foam method,α-naphthol-sulfuric acid precipitation method,acetic anhydride and sulfuric acid method for qualitative analysis of total saponin content,weight method and bromine method for quantitative analysis in each part of the Hovenia dulcis (including the leaves,branches,fruit,fruit residue,seed,shell),according to the total saponin extracting rate,the extracting techniques,including extracting temperature,solid to liquid ratio,extracting time were optimized by orthogonal design.The results showed that the total saponin content in stems was the highest.The sample was extracted by pure water,the extracting temperature was 60℃,the ratio of solid-solution was 1∶15 mg/L,the extracting time was 4.0 h(refluxing extraction for 1 times,2 h for each time),and the total extraction rate of Hovenia dulcis fruit was 16.5 mg/g.

References:

[1]Kawai K IAkiyama TOgihara Yet al.A new sapogenin in the saponins of Zizyphus jujubaHovenia dulcis and Bacopa monniera[J].Phytochemistry197413(12)2829-2832.

[2]吉川和子,津村慎一,山田恵子,等.Antisweet Natural Products.VII.Hodulosides IIIIIIIVand V from the leaves of Hovenia dulcisTHUNB[J].Chemical and Pharmaceutical Bulletin199240(9)2287-2291.

[3]Kimura YKobayashi YTakeda Tet al.Three new saponins from the leaves of Hovenia dulcis(Rhamnaceae)[J].J Chem Soc Perkin Trans1981(1)1923-1927.

[4]Yoshikawa KNagai YYoshida Met al.Antisweet natural products.VIII.Structures of hodulosides VI-X from Hovenia dulcisThunb.var.tomentella Makino[J].Chemical and Pharmaceutical Bulletin199341(10)1722-1725.

[5]梁侨丽,丁林生.枳椇叶化学成分研究 ()[J].中国药科大学学报,199627(7)401-404.

[6]Yoshikawa MMurakami TUeda Tet al.Bioactive saponins and glycosides.IV.Four methyl-migrated 1617-seco-dammarane triterpene glycosides from Chinese natural medicinehoveniae semen seu fructusthe seeds and fruit of Hovena dulcusTHUNB.Absolute stereostructures and inhibitory?activity on histamine release of hovenidulciosides A1A2B1and B2[J].Chemical and Pharmaceutical Bulletin199644(9)1736-1743.

[7]陈泉生.枳椇皂苷的药理性质[J].国外医学·药学分册,1980(1)45.

[8]石仁兵,李祥.中药化学[M].北京:科学出版社,2005.

[9]国家药典委员会.中华人民共和国药典[M].北京:中国医药出版社,2010.


Memo

Memo:
-
Last Update: 2014-08-27